By Houben J., Weyl T.
Methoden der Organischen Chemie (Methods of natural Chemistry, referred to as Houben-Weyl) is a customary reference paintings for chemists engaged in natural synthesis. In volumes on compound sessions, together with all Supplemental volumes, preparative equipment are taken care of comprehensively and severely. Tables of examples evaluate crucial tools and express their scope. precise experimental systems are given for the simplest equipment. The reactivity and extra reactions of every compound type also are provided. The large use of formulation schemes help in making the German-language volumes extra without difficulty comprehensible to non-German readers.
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Methoden der Organischen Chemie (Methods of natural Chemistry, known as Houben-Weyl) is a typical reference paintings for chemists engaged in natural synthesis. In volumes on compound sessions, together with all Supplemental volumes, preparative tools are handled comprehensively and significantly. Tables of examples evaluate an important equipment and express their scope.
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Extra resources for Houben-Weyl Methods in Organic Chemistry: Hetarenes: 6+ Membered Rings with 2+ Heteroatom
1). A high yield preparation of urethanes was reported from amides and DIB in methanolic potassium hydroxide : DIB MeOR KOH 70-97% RCONH2 -- RNHCOOMe A related reaction accompanied by cyclization occurred with ortho-substituted benzamides (and also non-cyclic amides such as RCH(CONH2)2 . Several compounds with a primary amino group, such as t-butylamine, p-toluenesulphonamide, ethyl carbamate, etc. were oxidized by DIB in presence of alkenes or nitroso compounds to give, respectively, aziridines or azoxy compounds.
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